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Advanced inorganic chemistry by Cotton F., Wilkinson G., Murillo C., Bochmann M.

By Cotton F., Wilkinson G., Murillo C., Bochmann M.

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Inorg. Organomet. 327 1H, 13C and 29Si NMR spectra were reported for (62), where R3 ¼ Me3, Me2Ph, MePh2, Ph3, Me2(OSiMe3). 336 1H, 13C 21 Spectrosc. Prop. Inorg. Organomet. 344 1H and 31P{1H} NMR spectra for (67), where M ¼ Rh or Ir, were reported. 348 31P NMR data were able to discriminate between enantiomers 22 Spectrosc. Prop. Inorg. Organomet. 353 2-D NMR experiments enabled a full characterisation of 4 isomers of [Ir(H)2{(S)-(R)L}(L 0 )]1, where L ¼ S-1-[(R-2-diphenylphosphanyl)ferrocenyl] ethyldi(3,5-xylyl)phosphane; L 0 ¼2,6-dimethylphenyl-1 0 -methyl-2 0 -methoxy354 1 31 ethylimine.

1 Carbon Compounds. 2 Silicon Compounds. 686 The proton NMR spectra of (Trip)SiH3 and (Trip)AsH2 (Trip ¼ triptycene) included a characteristic 41 Spectrosc. Prop. Inorg. Organomet. 699 NMR data were also reported for: silylarenes, Ar(SiH3)n, where Ar ¼ phenyl, tolyl, xylyl, n ¼ 1, 2 (1H, 29Si);700 t py F N (Me3Si)2Si Bu F Si C O C R OSiMe3 N Ph t Bu F PhCC BEt2 Me2Si py (142) t (143) (144) Bu B t Bu Me Si Me N BEt2 Me2Si N Me2M t Bu (145) B 2 (146) SiMe3 (147) 42 Spectrosc. Prop. Inorg. Organomet.

Prop. Inorg. Organomet. 353 2-D NMR experiments enabled a full characterisation of 4 isomers of [Ir(H)2{(S)-(R)L}(L 0 )]1, where L ¼ S-1-[(R-2-diphenylphosphanyl)ferrocenyl] ethyldi(3,5-xylyl)phosphane; L 0 ¼2,6-dimethylphenyl-1 0 -methyl-2 0 -methoxy354 1 31 ethylimine. 361 NMR data have also been reported for: Co3(CO)6[m2,Z2,Z1-C(Ph) C¼C(PPh2C(O)SC(O)](m2-PPh2) (31P);362 Co3(CO)9[m3-CCO2CH2CCH{Co4 (CO)10}] (1H);363 substituted m3-carbido-capped tricobalt carbonyl clusters (1H, 13C);364 Co(III) complexes of NH3, en, 1,2-propylenediamine or 1,2-cyclohexanediamine (1H, 13C, 59Co);365 [Co(CO)3(L)]À (L ¼ N,N-diethyl1,2-ethanediamine, N,N-bis(2-chloroethyl)-1,2-ethanediamine and related) (1H, 13C{1H});366 cis-[Co(en)2(N3)2]SCN (1H, 13C);367 (70), where R ¼ n-octyl, n-dodecyl, n-hexadecyl (1H, 13C);368 [CH2ClCo(tmsalen)]2, 3+ NH NH + H NH Co Cy P Ph3P Ir Co t Bu NH NH NH PPh3 (69) (70) R 23 Spectrosc.

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